Sammelbandbeitrag

SAXS analysis of mesoporous model materials : a validation of data evaluation techniques to characterize pore size, shape, surface area, and curvature of the interface


AutorenlisteSmarsly, B; Groenewolt, M; Antonietti, M

Erschienen inScattering Methods and the Properties of Polymer Materials

HerausgeberlisteStribeck, N; Smarsly, B

Jahr der Veröffentlichung2005

Seiten105-113

ISBN978-3-540-25323-5

eISBN978-3-540-31510-0

DOI Linkhttps://doi.org/10.1007/b107347

Auflage1. Auflage

SerientitelProgress in Colloid and Polymer Science

Serienzählung130


Abstract

Two model mesoporous silicas with cylindrical and spherical mesopore architectures were analyzed with SAXS, using evaluation principles introduced by Ruland. The comparison with sorption measurements and transmission electron microscopy revealed that suitable SAXS analysis methods are a very precise technique to determine a whole range of structural properties of two-phase systems with mesostructure, namely the characteristic size of both phases, the surface area, the curvature of the phase boundary, and – applying the so-called κ -ι formalism – even the type of mesophases under consideration.




Zitierstile

Harvard-ZitierstilSmarsly, B., Groenewolt, M. and Antonietti, M. (2005) SAXS analysis of mesoporous model materials : a validation of data evaluation techniques to characterize pore size, shape, surface area, and curvature of the interface, in Stribeck, N. and Smarsly, B. (eds.) Scattering Methods and the Properties of Polymer Materials. 1. Auflage. Berlin / Heidelberg: Springer-Verlag, pp. 105-113. https://doi.org/10.1007/b107347

APA-ZitierstilSmarsly, B., Groenewolt, M., & Antonietti, M. (2005). SAXS analysis of mesoporous model materials : a validation of data evaluation techniques to characterize pore size, shape, surface area, and curvature of the interface. In Stribeck, N., & Smarsly, B. (Eds.), Scattering Methods and the Properties of Polymer Materials (1. Auflage, pp. 105-113). Springer-Verlag. https://doi.org/10.1007/b107347


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