Journalartikel

In-situ structural investigation of non-stoichiometric HfO2-x films using quick-scanning extended X-ray absorption fine structure


AutorenlisteLiu, M; Leichtweiss, T; Janek, J; Martin, M

Jahr der Veröffentlichung2013

Seiten60-64

ZeitschriftThin Solid Films

Bandnummer539

ISSN0040-6090

DOI Linkhttps://doi.org/10.1016/j.tsf.2013.04.149

VerlagElsevier


Abstract
In this work, we report our results on the synthesis and structural characterization of hafnium oxide thin films prepared by means of pulsed laser deposition. During the deposition, different gas atmospheres (O-2, Ar, Ar/H-2) were used. Electron probe micro analysis and X-ray photoelectron spectroscopy measurements show that films deposited in Ar or Ar/H-2 are oxygen deficient, while films deposited in O-2 are stoichiometric. X-ray diffraction data confirm that the as-prepared films are amorphous and form the monoclinic HfO2 phase during annealing. In-situ quick-scanning extended X-ray absorption fine structure measurements carried out at elevated temperatures up to 440 degrees C showed an increase in the Hf-Hf order. From the time-resolved data the crystallization kinetics are extracted and analyzed using the Avrami model.



Autoren/Herausgeber




Zitierstile

Harvard-ZitierstilLiu, M., Leichtweiss, T., Janek, J. and Martin, M. (2013) In-situ structural investigation of non-stoichiometric HfO2-x films using quick-scanning extended X-ray absorption fine structure, Thin Solid Films, 539, pp. 60-64. https://doi.org/10.1016/j.tsf.2013.04.149

APA-ZitierstilLiu, M., Leichtweiss, T., Janek, J., & Martin, M. (2013). In-situ structural investigation of non-stoichiometric HfO2-x films using quick-scanning extended X-ray absorption fine structure. Thin Solid Films. 539, 60-64. https://doi.org/10.1016/j.tsf.2013.04.149


Zuletzt aktualisiert 2025-21-05 um 15:31