Journal article

Assessing the capabilities of direct analysis in real time mass spectrometry for 5-hydroxymethylfurfural quantitation in honey


Authors listChernetsova, E.S.; Morlock, G.E.

Publication year2012

Pages22-32

JournalInternational Journal of Mass Spectrometry

Volume number314

DOI Linkhttps://doi.org/10.1016/j.ijms.2012.01.012

PublisherElsevier


Abstract

The limitations of direct analysis in real time mass spectrometry (DART-MS) were shown with the example of 5-hydroxymethylfurfural (HMF) quantitation in honey. An accurate analyte quantitation was impossible because the carbohydrate matrix partially degraded to the analyte in the ionization region. However, at a decreased DART temperature of 150 degrees C, the DART-MS screening was possible using two spiked reference samples. The influence of instrumental parameters on the composition of the DART mass spectra for HMF and carbohydrates was investigated. Also, first data on scanning surface analysis with DART-MS were obtained giving rise for further studies in this direction. (c) 2012 Elsevier B.V. All rights reserved.




Citation Styles

Harvard Citation styleChernetsova, E. and Morlock, G. (2012) Assessing the capabilities of direct analysis in real time mass spectrometry for 5-hydroxymethylfurfural quantitation in honey, International journal of mass spectrometry, 314, pp. 22-32. https://doi.org/10.1016/j.ijms.2012.01.012

APA Citation styleChernetsova, E., & Morlock, G. (2012). Assessing the capabilities of direct analysis in real time mass spectrometry for 5-hydroxymethylfurfural quantitation in honey. International journal of mass spectrometry. 314, 22-32. https://doi.org/10.1016/j.ijms.2012.01.012


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