Journalartikel

Jahr der Veröffentlichung: 2009

Seiten: 3300-3304

Zeitschrift: Physical Chemistry Chemical Physics

Bandnummer: 11

Heftnummer: 17

ISSN: 1463-9076

DOI Link: https://doi.org/10.1039/b822437d

Verlag: Royal Society of Chemistry

Abstract: 
We report the preparation of nanoscale carbon-titanium carbide composites with carbide contents of up to 80 wt%. The synthesis yields single-crystalline TiC nanocubes 20-30 nm in diameter embedded in a hierarchical porous carbon matrix. These composites were generated in the form of cylindrical monoliths but can be produced in various shapes using modern sol-gel and nanocasting methods in conjunction with carbothermal reduction. The monolithic material is characterized by a combination of microscopy, diffraction and physisorption. Overall, the results presented in this work represent a concrete design template for the synthesis of non-oxidic nanoscale composites with high surface areas.

Harvard-Zitierstil: Sonnenburg, K., Smarsly, B. and Brezesinski, T. (2009) Non-oxidic nanoscale composites : single-crystalline titanium carbide nanocubes in hierarchical porous carbon monoliths, Physical Chemistry Chemical Physics, 11(17), pp. 3300-3304. https://doi.org/10.1039/b822437d

APA-Zitierstil: Sonnenburg, K., Smarsly, B., & Brezesinski, T. (2009). Non-oxidic nanoscale composites : single-crystalline titanium carbide nanocubes in hierarchical porous carbon monoliths. Physical Chemistry Chemical Physics. 11(17), 3300-3304. https://doi.org/10.1039/b822437d